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http://hdl.handle.net/1942/14979
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DC Field | Value | Language |
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dc.contributor.author | Thomas, Joice | - |
dc.contributor.author | Van Rossom, Wim | - |
dc.contributor.author | Van Hecke, Kristof | - |
dc.contributor.author | Van Meervelt, Luc | - |
dc.contributor.author | Smet, Mario | - |
dc.contributor.author | Dehaen, Wim | - |
dc.contributor.author | MAES, Wouter | - |
dc.date.accessioned | 2013-04-08T06:26:25Z | - |
dc.date.available | 2013-04-08T06:26:25Z | - |
dc.date.issued | 2013 | - |
dc.identifier.citation | SYNTHESIS-STUTTGART, 45 (6), p. 734-742 | - |
dc.identifier.issn | 0039-7881 | - |
dc.identifier.uri | http://hdl.handle.net/1942/14979 | - |
dc.description.abstract | Selenium-bridged heteracalixarenes were synthesized by convenient one-pot SNAr reactions starting from variously 2-substituted 4,6-dichloro-1,3,5-triazine building blocks. Reactions of these precursors with sodium hydroselenide afforded the selenacalix[3]triazines as the only macrocyclic products. Yields of the cyclotrimers were significantly increased by optimization of the macrocyclization conditions, the optimum parameters being dependent on the triazine functionalization pattern. X-ray diffraction studies allowed unambiguous identification of the structures and comparison with the solid-state features of analogous heteracalixarenes. | - |
dc.language.iso | en | - |
dc.publisher | GEORG THIEME VERLAG KG | - |
dc.subject.other | (hetera)calixarenes; macrocycles; selenium; 1,3,5-triazines; substituent effects | - |
dc.subject.other | Chemistry, Organic; (hetera)calixarenes; macrocycles; selenium; 1,3,5-triazines; substituent effects | - |
dc.title | Synthetic Protocols towards Selenacalix[3]triazines | - |
dc.type | Journal Contribution | - |
dc.identifier.epage | 742 | - |
dc.identifier.issue | 6 | - |
dc.identifier.spage | 734 | - |
dc.identifier.volume | 45 | - |
local.format.pages | 9 | - |
local.bibliographicCitation.jcat | A1 | - |
dc.description.notes | [Thomas, Joice; Van Rossom, Wim; Van Hecke, Kristof; Van Meervelt, Luc; Smet, Mario; Dehaen, Wim; Maes, Wouter] Katholieke Univ Leuven, Dept Chem, B-3001 Louvain, Belgium. [Van Hecke, Kristof] Univ Ghent, Dept Inorgan & Phys Chem, B-9000 Ghent, Belgium. [Maes, Wouter] Hasselt Univ, Inst Mat Res IMO IMOMEC, B-3590 Diepenbeek, Belgium. | - |
local.publisher.place | STUTTGART | - |
local.type.refereed | Refereed | - |
local.type.specified | Article | - |
dc.identifier.doi | 10.1055/s-0032-1318265 | - |
dc.identifier.isi | 000315619600004 | - |
item.contributor | Thomas, Joice | - |
item.contributor | Van Rossom, Wim | - |
item.contributor | Van Hecke, Kristof | - |
item.contributor | Van Meervelt, Luc | - |
item.contributor | Smet, Mario | - |
item.contributor | Dehaen, Wim | - |
item.contributor | MAES, Wouter | - |
item.accessRights | Closed Access | - |
item.fulltext | No Fulltext | - |
item.fullcitation | Thomas, Joice; Van Rossom, Wim; Van Hecke, Kristof; Van Meervelt, Luc; Smet, Mario; Dehaen, Wim & MAES, Wouter (2013) Synthetic Protocols towards Selenacalix[3]triazines. In: SYNTHESIS-STUTTGART, 45 (6), p. 734-742. | - |
item.validation | ecoom 2014 | - |
crisitem.journal.issn | 0039-7881 | - |
crisitem.journal.eissn | 1437-210X | - |
Appears in Collections: | Research publications |
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