Please use this identifier to cite or link to this item: http://hdl.handle.net/1942/14979
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dc.contributor.authorThomas, Joice-
dc.contributor.authorVan Rossom, Wim-
dc.contributor.authorVan Hecke, Kristof-
dc.contributor.authorVan Meervelt, Luc-
dc.contributor.authorSmet, Mario-
dc.contributor.authorDehaen, Wim-
dc.contributor.authorMAES, Wouter-
dc.date.accessioned2013-04-08T06:26:25Z-
dc.date.available2013-04-08T06:26:25Z-
dc.date.issued2013-
dc.identifier.citationSYNTHESIS-STUTTGART, 45 (6), p. 734-742-
dc.identifier.issn0039-7881-
dc.identifier.urihttp://hdl.handle.net/1942/14979-
dc.description.abstractSelenium-bridged heteracalixarenes were synthesized by convenient one-pot SNAr reactions starting from variously 2-substituted 4,6-dichloro-1,3,5-triazine building blocks. Reactions of these precursors with sodium hydroselenide afforded the selenacalix[3]triazines as the only macrocyclic products. Yields of the cyclotrimers were significantly increased by optimization of the macrocyclization conditions, the optimum parameters being dependent on the triazine functionalization pattern. X-ray diffraction studies allowed unambiguous identification of the structures and comparison with the solid-state features of analogous heteracalixarenes.-
dc.language.isoen-
dc.publisherGEORG THIEME VERLAG KG-
dc.subject.other(hetera)calixarenes; macrocycles; selenium; 1,3,5-triazines; substituent effects-
dc.subject.otherChemistry, Organic; (hetera)calixarenes; macrocycles; selenium; 1,3,5-triazines; substituent effects-
dc.titleSynthetic Protocols towards Selenacalix[3]triazines-
dc.typeJournal Contribution-
dc.identifier.epage742-
dc.identifier.issue6-
dc.identifier.spage734-
dc.identifier.volume45-
local.format.pages9-
local.bibliographicCitation.jcatA1-
dc.description.notes[Thomas, Joice; Van Rossom, Wim; Van Hecke, Kristof; Van Meervelt, Luc; Smet, Mario; Dehaen, Wim; Maes, Wouter] Katholieke Univ Leuven, Dept Chem, B-3001 Louvain, Belgium. [Van Hecke, Kristof] Univ Ghent, Dept Inorgan & Phys Chem, B-9000 Ghent, Belgium. [Maes, Wouter] Hasselt Univ, Inst Mat Res IMO IMOMEC, B-3590 Diepenbeek, Belgium.-
local.publisher.placeSTUTTGART-
local.type.refereedRefereed-
local.type.specifiedArticle-
dc.identifier.doi10.1055/s-0032-1318265-
dc.identifier.isi000315619600004-
item.contributorThomas, Joice-
item.contributorVan Rossom, Wim-
item.contributorVan Hecke, Kristof-
item.contributorVan Meervelt, Luc-
item.contributorSmet, Mario-
item.contributorDehaen, Wim-
item.contributorMAES, Wouter-
item.accessRightsClosed Access-
item.fulltextNo Fulltext-
item.fullcitationThomas, Joice; Van Rossom, Wim; Van Hecke, Kristof; Van Meervelt, Luc; Smet, Mario; Dehaen, Wim & MAES, Wouter (2013) Synthetic Protocols towards Selenacalix[3]triazines. In: SYNTHESIS-STUTTGART, 45 (6), p. 734-742.-
item.validationecoom 2014-
crisitem.journal.issn0039-7881-
crisitem.journal.eissn1437-210X-
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