Please use this identifier to cite or link to this item: http://hdl.handle.net/1942/24153
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dc.contributor.authorTASSI, Marco-
dc.contributor.authorRoevens, Annelore-
dc.contributor.authorREEKMANS, Gunter-
dc.contributor.authorVANHAMEL, Martine-
dc.contributor.authorMeynen, Vera-
dc.contributor.authorD'HAEN, Jan-
dc.contributor.authorADRIAENSENS, Peter-
dc.contributor.authorCARLEER, Robert-
dc.date.accessioned2017-08-08T07:38:12Z-
dc.date.available2017-08-08T07:38:12Z-
dc.date.issued2017-
dc.identifier.citationADVANCED POWDER TECHNOLOGY, 28(1), p. 236-243-
dc.identifier.issn0921-8831-
dc.identifier.urihttp://hdl.handle.net/1942/24153-
dc.description.abstractThe microwave assisted reaction between P25 titanium dioxide (TiO2) and phenylphosphonic acid (PPA) is explored thoroughly and the influence of the reaction conditions on the grafting mechanism and formed products is presented. While the surface grafting is observed at low temperatures and water free conditions, the formation of titaniumphosphonate is favored in water and high reaction temperatures. For the first time the correlation between the amorphous TiO2 phase and the formation of titani-umphenylphosphonate is reported. Materials are fully characterized by attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR), solid-state P-31 Nuclear Magnetic Resonance (P-31 NMR) spectroscopy, energy dispersive X-ray (EDX) spectroscopy and transmission electron microscopy (TEM). (C) 2016 The Society of Powder Technology Japan. Published by Elsevier B.V. and The Society of Powder Technology Japan. All rights reserved.-
dc.description.sponsorshipThis work is financially supported by the Fund for Scientific Research of Flanders (FWO-Vlaanderen) via the project G. O127.12N. We further acknowledge the financial support from the Interuniversity Attraction Poles Programme (P7/05) initiated by the Belgian Science Policy Office (BELSPO).-
dc.language.isoen-
dc.publisherELSEVIER SCIENCE BV-
dc.rights(C) 2016 The Society of Powder Technology Japan. Published by Elsevier B.V. and The Society of Powder Technology Japan. All rights reserved.-
dc.subject.otherTiO2 surface modification; Titaniumphenylphosphonate; ATR-FTIR; P-31 solid state NMR; TEM; Phosphonic acid-
dc.subject.otherTiO2 surface modification; titaniumphenylphosphonate; ATR-FTIR; 31P solid state NMR; TEM; phosphonic acid-
dc.titleA detailed investigation of the microwave assisted phenylphosphonic acid modification of P25 TiO2-
dc.typeJournal Contribution-
dc.identifier.epage243-
dc.identifier.issue1-
dc.identifier.spage236-
dc.identifier.volume28-
local.format.pages8-
local.bibliographicCitation.jcatA1-
dc.description.notes[Tassi, Marco; Reekmans, Gunter; Vanhamel, Martine; D'Haen, Jan; Adriaensens, Peter; Carleer, Robert] Hasselt Univ, Appl & Analyt Chem, Inst Mat Res IMO, Agoralaan 1 Bldg D, B-3590 Diepenbeek, Belgium. [Roevens, Annelore; Meynen, Vera] Univ Antwerp, Lab Adsorpt & Catalysis, Univ Pl 1, B-2610 Antwerp, Belgium.-
local.publisher.placeAMSTERDAM-
local.type.refereedRefereed-
local.type.specifiedArticle-
dc.identifier.doi10.1016/j.apt.2016.09.020-
dc.identifier.isi000395355100027-
item.contributorTASSI, Marco-
item.contributorRoevens, Annelore-
item.contributorREEKMANS, Gunter-
item.contributorVANHAMEL, Martine-
item.contributorMeynen, Vera-
item.contributorD'HAEN, Jan-
item.contributorADRIAENSENS, Peter-
item.contributorCARLEER, Robert-
item.validationecoom 2018-
item.fullcitationTASSI, Marco; Roevens, Annelore; REEKMANS, Gunter; VANHAMEL, Martine; Meynen, Vera; D'HAEN, Jan; ADRIAENSENS, Peter & CARLEER, Robert (2017) A detailed investigation of the microwave assisted phenylphosphonic acid modification of P25 TiO2. In: ADVANCED POWDER TECHNOLOGY, 28(1), p. 236-243.-
item.accessRightsOpen Access-
item.fulltextWith Fulltext-
crisitem.journal.issn0921-8831-
crisitem.journal.eissn1568-5527-
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