Please use this identifier to cite or link to this item: http://hdl.handle.net/1942/2517
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dc.contributor.authorHARDY, An-
dc.contributor.authorMONDELAERS, Dirk-
dc.contributor.authorVANHOYLAND, Geert-
dc.contributor.authorVAN BAEL, Marlies-
dc.contributor.authorMULLENS, Jules-
dc.contributor.authorVAN POUCKE, Lucien-
dc.date.accessioned2007-11-15T09:15:27Z-
dc.date.available2007-11-15T09:15:27Z-
dc.date.issued2003-
dc.identifier.citationJOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, 26(1-3). p. 1103-1107-
dc.identifier.issn0928-0707-
dc.identifier.urihttp://hdl.handle.net/1942/2517-
dc.description.abstractBismuth titanate (Bi4Ti3O12) was synthesized by an aqueous solution-gel process starting from solutions of bismuth acetate and a peroxocitrato-Ti(IV) complex. To gain insight into the thermal decomposition pattern of the gel several thermal analysis techniques were employed: DTA, TGA-EGA (evolved gas analysis by on-line coupling to a FTIR or mass spectrometer) and HT-DRIFT. Transmission electron micrographs showed that the gel is chemically homogeneous down to ca. 5 nm and that this homogeneity is preserved throughout the heat treatment. High-temperature X-ray diffraction measurements were used to make an in situ study of the phase formation. It has been found that single phase Bi4Ti3O12 is formed at 625degreesC.-
dc.language.isoen-
dc.publisherKLUWER ACADEMIC PUBL-
dc.subject.otherBi4Ti3O12; aqueous solution-gel; thermal analysis; TEM; HT-XRD-
dc.titleThe formation of ferroelectric bismuth titanate (Bi4Ti3O12) from an aqueous metal-chelate gel-
dc.typeJournal Contribution-
dc.identifier.epage1107-
dc.identifier.issue1-3-
dc.identifier.spage1103-
dc.identifier.volume26-
local.format.pages5-
local.bibliographicCitation.jcatA1-
dc.description.notesLimburgs Univ Ctr, IMO, Lab Inorgan & Phys Chem, B-3590 Diepenbeek, Belgium.Mullens, J, Limburgs Univ Ctr, IMO, Lab Inorgan & Phys Chem, Univ Campus, B-3590 Diepenbeek, Belgium.-
local.type.refereedRefereed-
local.type.specifiedArticle-
dc.bibliographicCitation.oldjcatA1-
dc.identifier.doi10.1023/A:1020762824990-
dc.identifier.isi000178789100204-
item.fulltextNo Fulltext-
item.accessRightsClosed Access-
item.contributorMONDELAERS, Dirk-
item.contributorVANHOYLAND, Geert-
item.contributorVAN POUCKE, Lucien-
item.contributorHARDY, An-
item.contributorMULLENS, Jules-
item.contributorVAN BAEL, Marlies-
item.fullcitationHARDY, An; MONDELAERS, Dirk; VANHOYLAND, Geert; VAN BAEL, Marlies; MULLENS, Jules & VAN POUCKE, Lucien (2003) The formation of ferroelectric bismuth titanate (Bi4Ti3O12) from an aqueous metal-chelate gel. In: JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, 26(1-3). p. 1103-1107.-
item.validationecoom 2003-
crisitem.journal.issn0928-0707-
crisitem.journal.eissn1573-4846-
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