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http://hdl.handle.net/1942/2731
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DC Field | Value | Language |
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dc.contributor.author | VANHOYLAND, Geert | - |
dc.contributor.author | Bouree, F | - |
dc.contributor.author | VAN BAEL, Marlies | - |
dc.contributor.author | MULLENS, Jules | - |
dc.contributor.author | VAN POUCKE, Lucien | - |
dc.date.accessioned | 2007-11-15T21:48:40Z | - |
dc.date.available | 2007-11-15T21:48:40Z | - |
dc.date.issued | 2001 | - |
dc.identifier.citation | JOURNAL OF SOLID STATE CHEMISTRY, 157(2). p. 283-288 | - |
dc.identifier.issn | 0022-4596 | - |
dc.identifier.uri | http://hdl.handle.net/1942/2731 | - |
dc.description.abstract | The structure of acid strontium oxalate Sr(HC2O4) . 1/2(C2O4) . H2O has been determined by conventional X-ray powder diffractometry, The diffraction pattern was indexed from a monoclinic unit cell with cell parameters a = 6.341(1) Angstrom, b = 16.880(2) Angstrom, c = 5.7798(8) Angstrom, and beta = 97.60(1)degrees; space group, P2(1)/n (No. 14) with Z = 4. Final (isotropic) Rietveld refinement of the neutron powder data yielded R-B = 4.57%, R-F = 2.87%, and R-WP = 7.87% as conventional Rietveld parameters. Strontium is eight-fold coordinated and can be described as a distorted bicapped trigonal prism. The SrO8 polyhedra form one-dimensional chains along the c-axis bf sharing edges, In contrast to all other known strontium oxalates, in this compound H2O acts as bridging ligand between two Sr atoms, SDPD-D classification (1): Sr(HC2O4)-1/2(C2O4)-H2O, P2(1)/n, C1=14, Nc = 42, C2 = 11, XC1 + N/TREOR-97 & DICVOL-91, EXTRA, EQUI, SIRPOW-92 (DM), GFOURIER, FULLPROF, (C) 2001 Academic Press. | - |
dc.language.iso | en | - |
dc.publisher | ACADEMIC PRESS INC | - |
dc.subject.other | X-ray powder diffraction; neutron powder diffraction; oxalate; structure determination; Rietveld refinement | - |
dc.title | Structure determination and refinement of acid strontium oxalate from X-ray and neutron powder diffraction | - |
dc.type | Journal Contribution | - |
dc.identifier.epage | 288 | - |
dc.identifier.issue | 2 | - |
dc.identifier.spage | 283 | - |
dc.identifier.volume | 157 | - |
local.format.pages | 6 | - |
local.bibliographicCitation.jcat | A1 | - |
dc.description.notes | Limburgs Univ Ctr, IMO, Lab Inorgan & Phys Chem, B-3590 Diepenbeek, Belgium. CEA Saclay, CNRS, Leon Brillouin Lab, F-91191 Gif Sur Yvette, France.Vanhoyland, G, Limburgs Univ Ctr, IMO, Lab Inorgan & Phys Chem, Univ Campus, B-3590 Diepenbeek, Belgium. | - |
local.type.refereed | Refereed | - |
local.type.specified | Article | - |
dc.bibliographicCitation.oldjcat | A1 | - |
dc.identifier.doi | 10.1006/jssc.2000.9057 | - |
dc.identifier.isi | 000167791600006 | - |
item.accessRights | Closed Access | - |
item.contributor | VANHOYLAND, Geert | - |
item.contributor | Bouree, F | - |
item.contributor | VAN BAEL, Marlies | - |
item.contributor | MULLENS, Jules | - |
item.contributor | VAN POUCKE, Lucien | - |
item.fulltext | No Fulltext | - |
item.fullcitation | VANHOYLAND, Geert; Bouree, F; VAN BAEL, Marlies; MULLENS, Jules & VAN POUCKE, Lucien (2001) Structure determination and refinement of acid strontium oxalate from X-ray and neutron powder diffraction. In: JOURNAL OF SOLID STATE CHEMISTRY, 157(2). p. 283-288. | - |
item.validation | ecoom 2002 | - |
crisitem.journal.issn | 0022-4596 | - |
crisitem.journal.eissn | 1095-726X | - |
Appears in Collections: | Research publications |
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