Please use this identifier to cite or link to this item: http://hdl.handle.net/1942/3133
Title: Sulphur group analysis in solid matrices by atmospheric pressure-temperature programmed reduction
Authors: YPERMAN, Jan 
MAES, Inge
VAN DEN RUL, Heidi 
MULLENS, Steven 
VAN AELST, Joke
FRANCO, Dirk 
MULLENS, Jules 
VAN POUCKE, Lucien 
Issue Date: 1999
Publisher: ELSEVIER SCIENCE BV
Source: ANALYTICA CHIMICA ACTA, 395(1-2). p. 143-155
Abstract: The atmospheric pressure-temperature programmed reduction (AP-TPR) has become an established and reliable method amongst the different sulphur characterisation techniques for solid materials, like coal and coal derived products, rubber and clay. The analytical method is based upon the fact that specific sulphur functional groups are hydrogenated at specific temperatures. During the last few years, several adjustments have been made to the hard- and software as well as to the experimental parameters. The changes and the reliability of the method are extensively discussed in this paper, (C) 1999 Elsevier Science B.V. All rights reserved.
Notes: Limburgs Univ Ctr, IMO, Lab Inorgan & Phys Chem, B-3590 Diepenbeek, Belgium.Yperman, J, Limburgs Univ Ctr, IMO, Lab Inorgan & Phys Chem, Univ Campus, B-3590 Diepenbeek, Belgium.
Keywords: sulphur determination; AP-TPR; hydrogenation; coal; rubber
Document URI: http://hdl.handle.net/1942/3133
DOI: 10.1016/S0003-2670(99)00362-1
ISI #: 000082103900015
Type: Journal Contribution
Validations: ecoom 2000
Appears in Collections:Research publications

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