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Title: | Sulphur group analysis in solid matrices by atmospheric pressure-temperature programmed reduction | Authors: | YPERMAN, Jan MAES, Inge VAN DEN RUL, Heidi MULLENS, Steven VAN AELST, Joke FRANCO, Dirk MULLENS, Jules VAN POUCKE, Lucien |
Issue Date: | 1999 | Publisher: | ELSEVIER SCIENCE BV | Source: | ANALYTICA CHIMICA ACTA, 395(1-2). p. 143-155 | Abstract: | The atmospheric pressure-temperature programmed reduction (AP-TPR) has become an established and reliable method amongst the different sulphur characterisation techniques for solid materials, like coal and coal derived products, rubber and clay. The analytical method is based upon the fact that specific sulphur functional groups are hydrogenated at specific temperatures. During the last few years, several adjustments have been made to the hard- and software as well as to the experimental parameters. The changes and the reliability of the method are extensively discussed in this paper, (C) 1999 Elsevier Science B.V. All rights reserved. | Notes: | Limburgs Univ Ctr, IMO, Lab Inorgan & Phys Chem, B-3590 Diepenbeek, Belgium.Yperman, J, Limburgs Univ Ctr, IMO, Lab Inorgan & Phys Chem, Univ Campus, B-3590 Diepenbeek, Belgium. | Keywords: | sulphur determination; AP-TPR; hydrogenation; coal; rubber | Document URI: | http://hdl.handle.net/1942/3133 | DOI: | 10.1016/S0003-2670(99)00362-1 | ISI #: | 000082103900015 | Type: | Journal Contribution | Validations: | ecoom 2000 |
Appears in Collections: | Research publications |
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