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http://hdl.handle.net/1942/36239
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DC Field | Value | Language |
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dc.contributor.author | VERSTRAETE, Kirsten | - |
dc.contributor.author | BUCKINX, Axel | - |
dc.contributor.author | ZAQUEN, Neomy | - |
dc.contributor.author | JUNKERS, Tanja | - |
dc.date.accessioned | 2021-12-16T12:09:37Z | - |
dc.date.available | 2021-12-16T12:09:37Z | - |
dc.date.issued | 2021 | - |
dc.date.submitted | 2021-08-27T10:40:04Z | - |
dc.identifier.citation | MACROMOLECULES, 54 (8) , p. 3865 -3872 | - |
dc.identifier.uri | http://hdl.handle.net/1942/36239 | - |
dc.description.abstract | Micelle dispersions purification is made available via inline flow dialysis in which micelles are separated from the organic solvent used to dissolve the block copolymers in the micelle formation step. Purification was performed using simple and cost-effective dialysis units employing cellulose membranes. The proposed setup allows us to remove THF from a micelle dispersion within a few hours almost entirely in a looped flow system, without significantly changing the micelle size. Purification is found to be independent of the exact flow rates and only on the circulation time through the dialysis units. The system is not only able to reduce the concentration of the organic solvent, but also water-soluble monomers can be removed. Further, the integration of the method into a full synthesis line to produce encapsulated micelles directly from block copolymer solutions is demonstrated with a throughput of 1.2 g of micelles per hour. | - |
dc.description.sponsorship | The authors are grateful for funding from Hasselt University and the Fonds Wetenschappelijk Onderzoek (FWO). Further, support of the project via a discovery project of the Australian Research Council (ARC) in the form of DP190103309 is kindly acknowledged. | - |
dc.language.iso | en | - |
dc.publisher | AMER CHEMICAL SOC | - |
dc.rights | 2021 American Chemical Society | - |
dc.title | Micelle Purification in Continuous Flow via Inline Dialysis | - |
dc.type | Journal Contribution | - |
dc.identifier.epage | 3872 | - |
dc.identifier.issue | 8 | - |
dc.identifier.spage | 3865 | - |
dc.identifier.volume | 54 | - |
local.bibliographicCitation.jcat | A1 | - |
local.publisher.place | 1155 16TH ST, NW, WASHINGTON, DC 20036 USA | - |
local.type.refereed | Refereed | - |
local.type.specified | Article | - |
dc.identifier.doi | 10.1021/acs.macromol.1c00242 | - |
dc.identifier.isi | 000645430100026 | - |
local.provider.type | Web of Science | - |
local.uhasselt.international | yes | - |
item.validation | ecoom 2022 | - |
item.fulltext | With Fulltext | - |
item.accessRights | Open Access | - |
item.fullcitation | VERSTRAETE, Kirsten; BUCKINX, Axel; ZAQUEN, Neomy & JUNKERS, Tanja (2021) Micelle Purification in Continuous Flow via Inline Dialysis. In: MACROMOLECULES, 54 (8) , p. 3865 -3872. | - |
item.contributor | VERSTRAETE, Kirsten | - |
item.contributor | BUCKINX, Axel | - |
item.contributor | ZAQUEN, Neomy | - |
item.contributor | JUNKERS, Tanja | - |
crisitem.journal.issn | 0024-9297 | - |
crisitem.journal.eissn | 1520-5835 | - |
Appears in Collections: | Research publications |
Files in This Item:
File | Description | Size | Format | |
---|---|---|---|---|
Template for Electronic Submission to ACS Journals.pdf | Peer-reviewed author version | 958.63 kB | Adobe PDF | View/Open |
Micelle Purification in Continuous Flow via Inline Dialysis.pdf Restricted Access | Published version | 2.55 MB | Adobe PDF | View/Open Request a copy |
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