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Title: | IMPROVING SELECTIVITY BY USING A MULTIPURPOSE CROSS-POLARIZATION MAGIC-ANGLE-SPINNING NMR PULSE SEQUENCE - CHARACTERIZATION OF PI-CONJUGATED COMPOUNDS | Authors: | HOOGMARTENS, I VANDERZANDE, Dirk ADRIAENSENS, Peter GELAN, Jan |
Issue Date: | 1993 | Publisher: | ELSEVIER SCIENCE BV | Source: | ANALYTICA CHIMICA ACTA, 283(3). p. 1025-1031 | Abstract: | The use of a multipurpose cross polarization magic angle spinning nuclear magnetic resonance pulse sequence to simplify high resolution solid state C-13 NMR spectra is reported. Several kinds of experiments such as cross polarization, cross depolarization, proton dipolar dephasing and combinations of these are demonstrated for the well characterized trans-3,3'-bibenzo[c]thienylidene-1,1'-d The pulse sequence is further applied to the analysis of insoluble poly(isothianaphthene). | Notes: | LIMBURGS UNIV CENTRUM,INST MAT RES,ORGAN CHEM RES GRP,B-3590 DIEPENBEEK,BELGIUM. | Keywords: | NUCLEAR MAGNETIC RESONANCE SPECTROMETRY; TRANS-3,3'-BIBENZO[C]THIENYLIDENE-1,1'-DIONE; SOLID STATE NMR | Document URI: | http://hdl.handle.net/1942/3643 | ISI #: | A1993MQ70800007 | Type: | Journal Contribution |
Appears in Collections: | Research publications |
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