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http://hdl.handle.net/1942/38002
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DC Field | Value | Language |
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dc.contributor.author | VANCLEEF, Arne | - |
dc.contributor.author | De Beuckeleer , Ward | - |
dc.contributor.author | Van Gerven , Tom | - |
dc.contributor.author | THOMASSEN, Leen | - |
dc.contributor.author | BRAEKEN, Leen | - |
dc.date.accessioned | 2022-09-07T10:01:43Z | - |
dc.date.available | 2022-09-07T10:01:43Z | - |
dc.date.issued | 2021 | - |
dc.date.submitted | 2022-08-16T16:18:22Z | - |
dc.identifier.citation | Processes, 9 (12) (Art N° 2268) | - |
dc.identifier.uri | http://hdl.handle.net/1942/38002 | - |
dc.description.abstract | Continuous tubular crystallizers have the potential to reduce manufacturing costs and increase product quality. However, designing tubular crystallizers is a complex and challenging task as crystallization is a complex, multiphase process with a propensity for fouling and clogging. While several designs have been proposed to overcome these issues, these designs are either unproven or poorly scalable and complex. In this work a continuous crystallizer is designed and evaluated to mitigate these issues. The tubular crystallizer combines a novel method to obtain a cubic cooling profile to control the supersaturation, ultrasound to induce nucleation and oscillatory flow to improve mixing and minimize fouling and sedimentation. The results show that the crystallizer was able to operate for more than 4 h without clogging, with high yields and a narrow particle size distribution. The design proposed here is therefore considered a viable approach for continuous crystallizers. | - |
dc.description.sponsorship | This research was funded by the Agency for Innovation and Entrepreneurship (VLAIO) and Catalisti Grant Number MMICAS HBC.2020.2627. | - |
dc.language.iso | en | - |
dc.publisher | MDPI | - |
dc.rights | 2021 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https:// creativecommons.org/licenses/by/ 4.0/). | - |
dc.subject.other | continuous crystallization | - |
dc.subject.other | tubular crystallizer | - |
dc.subject.other | oscillatory baffleless coil reactors | - |
dc.subject.other | pulsation | - |
dc.subject.other | oscillatory flow | - |
dc.subject.other | cubic cooling profile | - |
dc.subject.other | ultrasound assisted nucleation | - |
dc.subject.other | fouling | - |
dc.title | Continuous Crystallization Using Ultrasound Assisted Nucleation, Cubic Cooling Profiles and Oscillatory Flow | - |
dc.type | Journal Contribution | - |
dc.identifier.issue | 12 | - |
dc.identifier.volume | 9 | - |
local.bibliographicCitation.jcat | A1 | - |
dc.description.notes | Vancleef, A; Braeken, L (corresponding author), Katholieke Univ Leuven, Dept Chem Engn, Res Unit CIPT, Diepenbeek Campus,Agoralaan Gebouw B, B-3590 Diepenbeek, Belgium. | - |
dc.description.notes | arne.vancleef@kuleuven.be; ward.de.beuckeleer@hotmail.be; | - |
dc.description.notes | tom.vangerven@kuleuven.be; leen.thomassen@kuleuven.be; | - |
dc.description.notes | leen.braeken@kuleuven.be | - |
local.publisher.place | ST ALBAN-ANLAGE 66, CH-4052 BASEL, SWITZERLAND | - |
local.type.refereed | Refereed | - |
local.type.specified | Article | - |
local.bibliographicCitation.artnr | 2268 | - |
dc.identifier.doi | 10.3390/pr9122268 | - |
dc.identifier.isi | 000827228200001 | - |
dc.contributor.orcid | Van Gerven, Tom/0000-0003-2051-5696; Vancleef, Arne/0000-0001-6286-649X | - |
local.provider.type | wosris | - |
local.description.affiliation | [Vancleef, Arne; De Beuckeleer, Ward; Thomassen, Leen C. J.; Braeken, Leen] Katholieke Univ Leuven, Dept Chem Engn, Res Unit CIPT, Diepenbeek Campus,Agoralaan Gebouw B, B-3590 Diepenbeek, Belgium. | - |
local.description.affiliation | [Van Gerven, Tom] Katholieke Univ Leuven, Dept Chem Engn, Res Unit ProC, Celestijnenlaan 200F Box 2424, B-3001 Leuven, Belgium. | - |
local.uhasselt.international | no | - |
item.fulltext | With Fulltext | - |
item.fullcitation | VANCLEEF, Arne; De Beuckeleer , Ward; Van Gerven , Tom; THOMASSEN, Leen & BRAEKEN, Leen (2021) Continuous Crystallization Using Ultrasound Assisted Nucleation, Cubic Cooling Profiles and Oscillatory Flow. In: Processes, 9 (12) (Art N° 2268). | - |
item.accessRights | Open Access | - |
item.contributor | VANCLEEF, Arne | - |
item.contributor | De Beuckeleer , Ward | - |
item.contributor | Van Gerven , Tom | - |
item.contributor | THOMASSEN, Leen | - |
item.contributor | BRAEKEN, Leen | - |
crisitem.journal.eissn | 2227-9717 | - |
Appears in Collections: | Research publications |
Files in This Item:
File | Description | Size | Format | |
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Continuous Crystallization Using Ultrasound Assisted Nucleation, Cubic Cooling Profiles and Oscillatory Flow.pdf | Published version | 4.44 MB | Adobe PDF | View/Open |
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