Complete assignment of 1H and 13C NMR spectra of a set of sulphinyl and sulphonyl monomers towards poly(p-phenylene vinylene) precursors by 2D-NMR techniques

Please use this identifier to cite or link to this item: http://hdl.handle.net/1942/4534

Title:	Complete assignment of 1H and 13C NMR spectra of a set of sulphinyl and sulphonyl monomers towards poly(p-phenylene vinylene) precursors by 2D-NMR techniques
Authors:	VAN BREEMEN, ALBERT ADRIAENSENS, Peter Issaris, A.C.J. DE KOK, Margreet VANDERZANDE, Dirk GELAN, Jan
Issue Date:	2000
Publisher:	JOHN WILEY & SONS LTD
Source:	Magnetic resonance in chemistry, 38. p. 129-134
Abstract:	The complete assignment of the H-1 and C-13 NMR spectra of sulphinyl and sulphonyl monomers toward poly(p-phenylenevinylene) precursors is presented. For all compounds the same protocol could be used. Resonance assignments were achieved by the use of one- and two dimensional NMR techniques such as H-1, C-13 APT and 2D HETCOR (J = 8 Hz, J = 140 Hz), INADEQUATE and COSY. Copyright (C) 2000 John Wiley & Sons, Ltd.
Keywords:	NUCLEAR MAGNETIC-RESONANCE; NATURAL-ABUNDANCE SAMPLES; DOUBLE-QUANTUM COHERENCE; TWO-DIMENSIONAL NMR; SYNTHETIC ROUTE; POLYMER DIODES; DERIVATIVES; COUPLINGS; MOBILITY; NMR; H-1 NMR; C-13 NMR; 2D NMR; COSY; HETCOR; INADEQUATE; conjugated polymers; poly(p-phenylenevinylene); sulphinyl precursor route
Document URI:	http://hdl.handle.net/1942/4534
DOI:	10.1002/(SICI)1097-458X(200002)38:2<129::AID-MRC602>3.0.CO;2-K
ISI #:	000085269000009
Category:	A1
Type:	Journal Contribution
Validations:	ecoom 2001
Appears in Collections:	Research publications

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