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Title: | Complete assignment of 1H and 13C NMR spectra of a set of sulphinyl and sulphonyl monomers towards poly(p-phenylene vinylene) precursors by 2D-NMR techniques | Authors: | VAN BREEMEN, ALBERT ADRIAENSENS, Peter Issaris, A.C.J. DE KOK, Margreet VANDERZANDE, Dirk GELAN, Jan |
Issue Date: | 2000 | Publisher: | JOHN WILEY & SONS LTD | Source: | Magnetic resonance in chemistry, 38. p. 129-134 | Abstract: | The complete assignment of the H-1 and C-13 NMR spectra of sulphinyl and sulphonyl monomers toward poly(p-phenylenevinylene) precursors is presented. For all compounds the same protocol could be used. Resonance assignments were achieved by the use of one- and two dimensional NMR techniques such as H-1, C-13 APT and 2D HETCOR (J = 8 Hz, J = 140 Hz), INADEQUATE and COSY. Copyright (C) 2000 John Wiley & Sons, Ltd. | Keywords: | NUCLEAR MAGNETIC-RESONANCE; NATURAL-ABUNDANCE SAMPLES; DOUBLE-QUANTUM COHERENCE; TWO-DIMENSIONAL NMR; SYNTHETIC ROUTE; POLYMER DIODES; DERIVATIVES; COUPLINGS; MOBILITY; NMR; H-1 NMR; C-13 NMR; 2D NMR; COSY; HETCOR; INADEQUATE; conjugated polymers; poly(p-phenylenevinylene); sulphinyl precursor route | Document URI: | http://hdl.handle.net/1942/4534 | DOI: | 10.1002/(SICI)1097-458X(200002)38:2<129::AID-MRC602>3.0.CO;2-K | ISI #: | 000085269000009 | Category: | A1 | Type: | Journal Contribution | Validations: | ecoom 2001 |
Appears in Collections: | Research publications |
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