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http://hdl.handle.net/1942/25890
Title: | Photo-induced ring-closure via a looped flow reactor | Authors: | BAETEN, Evelien RUBENS, Maarten Wuest, Kilian N.R. Barner-Kowollik, Christopher JUNKERS, Tanja |
Issue Date: | 2017 | Source: | Reaction Chemistry & Engineering, 2(6), p. 826-829 | Abstract: | Looped flow processes are an efficient and versatile tool to synthesize complex macromolecular materials. Especially for light-induced ring-closure reactions, which typically require low concentrations, looped flow processes are critical for upscaling. Here, such a reactor was designed to carry out a photo-induced ring-closure reaction via a photo-enol reaction for the synthesis of cyclic polymers, leading to a reduction of required solvent in the synthesis by over a factor of 40, hence giving access to a more economical and fully scalable process. | Keywords: | looped flow processes; light-induced ring-closure reactions; photo-enol reaction; cyclic polymers; synthesis | Document URI: | http://hdl.handle.net/1942/25890 | ISSN: | 2058-9883 | e-ISSN: | 2058-9883 | DOI: | 10.1039/C7RE00124 | Rights: | This journal is © The Royal Society of Chemistry 2017 | Category: | A2 | Type: | Journal Contribution |
Appears in Collections: | Research publications |
Files in This Item:
File | Description | Size | Format | |
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c7re00124j.pdf Restricted Access | Published version | 890.49 kB | Adobe PDF | View/Open Request a copy |
cyclic polymersloop flow_FINAL.pdf | Peer-reviewed author version | 1.01 MB | Adobe PDF | View/Open |
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